The present study presented an integrated analytical approach to the Qur’anic manuscript with leather binding; the multianalyses revealed the degree of degradation for paper and leather in the current manuscript under the study, causing the mapping of treatment. The visual assessment detected yellowness in the internal papers, dark black spots, and advanced erosion in the leather bind. The result detected that this manuscript leads to yellowing and weakness in the properties of paper under the attack of acidity where the pH of paper reached 5.5. XRD and FTIR analyses of paper illustrated a dramatic decrease of crystallinity index with a notable increase of C=O stretching, respectively. The sharp increase of carbonyl group can be used as evidence of oxidation. The microscopic examination also showed that cotton was used in the manufacturing of the paper of the current manuscript, while the leather bind was made from goatskin. In addition, the cellulose and protein bundles were both destructive and disintegrated.
Corn grains were steeped in fresh SO2 solution (300 ppm), old SO2 solution (100 ppm, 0.55 g lactic acid per 100 ml) and fresh SO2 with chemically pure lactic acid (100 ppm SO2 + 0.55 g lactic acid per 100 ml). The water absorption rate in all trials using old SO2 or low SO2 with lactic acid in the first stage of the steeping process was higher. The solubilization and diffusion of protein was stronger in corn grains steeped completely in old SO2 or low fresh SO2 with lactic acid. Such treatments gave the highest starch recovery with lowest protein content in the isolated starch. The low starch content in hulls and fibers confirms the important role of lactic acid in presence of a low concentration of SO2 (0.01%).
The reaction of compounds 1, 2, 3, 4, or 13 with 2-chloroethyl methyl ether or 2,3,4,6-tetra-O-acetyl-alpha-D-glucopyranosyl bromide, afforded some acyclic and cyclic nucleosides of thieno[2,3-d]pyrimidine derivatives. Furthermore, cyclic C-nucleosides 24 and 25 were prepared from the reaction of 20, 21 or from 26, 27 with D-glucose. The antimicrobial evaluation of some prepared products showed promising antimicrobial activity.
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