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A new enantiomerically pure potential toxaphene congener (C10H9Cl9) has been isolated from a reaction mixture obtained by the free radical chlorination of (1S)‐2‐endo‐chloro­bornane and its absolute configuration determined. It crystallizes in the monoclinic space group C2 with two mol­ecules in the asymmetric unit. This is the first report of the preparation of a single enantiomer of a synthetic poly­chloro­terpene on a multi‐milligram scale.