Das Chlormethyl‐dimethylchlorsilan (I) reagiert leicht mit Alkoholen (II) ohne HCl‐Akzeptor zu den farblosen, flüssigen Chlormethyl‐dimethylalkoxysilanen (III), auf die man Kaliumacetat (IV) bei 140°C einwirken läßt. Dabei entstehen die gesuchten Acetoxymethyl‐dimethylalkoxysilane (V).
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