Durch Halogenierung von Pentamethylphenol mit ClO3F (in Pyridin bei 25°C), tert.‐Butylhypochlorit (in Pyridin bei 0°C) bzw. Brom (in Diäthyläther‐Pyridin bei ‐40°C) werden die Halogencyclohexadienone (I) (Ausbeute 14, 42 bzw. 63%) dargestellt.
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