Fe/ Ag granular multilayers were examined by magnetization and Mössbauer spectroscopy measurements. Very-thin ͑0.2 nm͒ discontinuous Fe layers show superparamagnetic properties that can be tailored by the thickness of both the magnetic and the spacer layers. Novel heterostructures, superparamagnetic and ferromagnetic layers stacked in different sequences, were prepared and the specific contribution of the ferromagnetic layers to the low-field magnetic susceptibility was identified.

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