Reductions of compounds whose benzylic positions bear O-atoms, such as benzyl alcohol, dibenzyl ether, styrene oxide, benzaldehyde, acetophenone, and benzophenone, to the corresponding nonconjugated dienes were performed by using t-BuOH, Li, and gaseous NH 3 in THF at room temperature. In these reductions, it was observed that the functional groups at benzylic positions were reduced first.
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