Fourier transform infrared spectroscopy and imaging coupled to optical microscopy, scanning electron microscopy coupled to energy dispersive x-ray spectroscopy and high-performance liquid chromatography (HPLC) coupled to diode-array detection are used to investigate two samples removed from a painted decoration of a burial kline and a textile fragment, both found in Koru tumulus (fifth century BCE) in Daskyleion. Tyrian purple and kaolinite were identified in both samples, thus suggesting that the aluminosilicate compound had an important role in the applied painting and dyeing processes. The textile fragment is composed of undyed cotton and silk yarns dyed with the molluskan dye. The relative compositions of the molluskan materials used in the two archaeological objects are similar and comparable with the corresponding composition measured for a purple sample originated from Murex trunculus mollusks according to the HPLC results. This result is supported by principal component analysis (PCA) which, furthermore, takes into account the relative compositions of the extracts of the three Mediterranean mollusks, published in previous reports.

A biological object was recovered from the pelvic region of an adult woman coded to SK13 unearthed from Oluz Höyük in Amasya, Turkey. The skeleton was dated to the medieval period on the basis of the burial customs and the calibrated 14C dates. The find was identified as a bladder stone on morphological, radiographic and chemo‐analytical grounds with the help of X‐ray diffraction, polarised energy dispersive X‐ray fluorescence spectroscopy, confocal Raman spectroscopy, and microscopic techniques. The mineralogical composition of urinary stone was found to be as calcium phosphate (apatite). Bladder stone disease is endemic in poor agricultural regions where the typical diet is mostly based on grain carbohydrate consumption with scarce intake of animal protein. Copyright © 2013 John Wiley & Sons, Ltd.

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