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the S 0 dissolving capacity of SO 2 , CS 2 , and CCl 4 are 0.015, 28.45 and 1.25%(w/v), respectively. Since the solubility of S 0 is higher in CS 2 , Mishra et al. 31 and Kim et al. 32 have used it as the solvent to remove the S 0 present in SC, though they have not studied its advantage on Mo leaching in details. Issues related to the Mo leaching from a SC sample are sorted out on the basis of leaching experiments in this paper. The main objective of experiments is the complete Mo dissolution in a single step instead of a multi-step leaching process by addressing the obstructions. The extraction, separation, and concentration enrichment of Mo and V from the leach liquor is reported. Finally a process flow-diagram is suggested.