This study presents the results of the synthesis of silver chloride nanoparticles dispersed within ammonium nitrate matrix via displacement mechanochemical reaction NH4Cl + AgNO3 + zNH4NO3 = (z + 1)NH4NO3 + AgCl at z = z1 = 7.22 and z = z2 = 3.64. The intermediate compound, NH4Ag(NO3)2, was identied after mechanochemical processing of studied system. Use of simultaneous thermogravimetry and dierential scanning calorimetry provide a new means for preparing silver chloride nanoparticles in their free form by thermal treatment.

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