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The 4-pentylphenyl-4'-pentox thiobenzoate (5S5), C,,H,,O,S, cr stallizes in the monoclinic system: space group P2,/c, a = 19.817 (2) 1, b = 5.585 (1) A, c = 20.238 (2) = 104.792 (8)', z = 4. The structure was solved by direct methods and refined to the final R=0.065, for 3415 observed reflections. The pentoxythiobezoate moiety is nearly planer. Molecular rows form an interclated structure. C-H ... 0 type short intermolecular contacts were found.

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