The Present work outlines the antibacterial activity of Fe 3 O 4 nanoparticles synthesized through chemical combustion method where ferric nitrate is used as precursor material and urea as fuel with the assistant of Tween 80, a non-ionic surfactant. The obtained Fe 3 O 4 nanoparticles were characterized by X-ray diffraction, differential thermal analysis/thermo gravimetric analysis (DTA/TGA), particle size analyzer, SEM with EDAX and TEM. Various parameters such as dislocation density, micro strain, analysis of weight loss and surface morphological studies were calculated. The particle size was calculated from XRD and it was found to be 33-40 nm. Using well diffusion method antibacterial activity of Fe 3 O 4 nanoparticles was tested against gram-positive and gramnegative Staphylococus aureus, Xanthomonas, Escherichia coli and Proteus vulgaris. Fe 3 O 4 nanoparticles exhibited strong antibacterial activity against bacterial species.
Zinc oxide nano powder synthesis is carried by a single step simple and fast combustion method using Zinc nitrate as precursor, HMTA as fuel material and non-ionic surfactant (Triton-X 100). The X-Ray diffraction (XRD) analysis revealed that the synthesized ZnO nanopowder has the pure wurtzite structure. The ZnO powder shows polycrystalline nature having the crystallite size 21.25 nm. Crystallite size is calculated using Debye-Scherrer's and Williamson-Hall equations. Porosity, Cell Volume, Micro strain, Morphology Index, Lorentz factor and Lorentz Polarization factor are also studied. From differential thermal analysis (DTA) & thermo gravimetric (TGA) it has been confirmed that nano powder has the phase purity. The weight loss percentage of the sample is 2.8385%. The particle size obtained 29 nm is in good agreement with the crystallite size calculated from X-Ray Diffraction pattern with the Particle Size Analyzer. The morphology of as prepared Zinc oxide nanopowders are characterized by scanning electron microscope (SEM). From specific area electron diffraction (SAED) pattern has specified the d-spacing and corresponding planes which coincide with the XRD d-spacing and planes.
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