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A montmorillonite has been intercalated with Al3+ polycations, using concentrated solutions and clay mineral dispersions. The reaction has been assisted by microwave radiation, yielding new intercalated solids and leading to Al-pillared solids after their calcination at 500 °C. The solids were characterized by elemental chemical analysis, X-ray diffraction, FTIR spectroscopy, thermal analyses, and nitrogen adsorption. The evolution of the properties of the materials was discussed as a function of the preparation conditions. Microwave treatment for 2.5 min provided correctly pillared solids.

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Two synthesis approaches of Fe-containing intercalated montmorillonites: Differences as acid catalysts for the synthesis of 1,5-benzodeazepine from 1,2-phenylenediamine and acetone

González

Trujillano

Vicente

et al. 2017

Applied Clay Science

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Beatriz González

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Two synthesis approaches of Fe-containing intercalated montmorillonites: Differences as acid catalysts for the synthesis of 1,5-benzodeazepine from 1,2-phenylenediamine and acetone

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