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Dynamics of segregation and fluidization of unary particles and binary mixtures in a cylindrical fluidized bed is investigated using temporally– and spatially–resolved measurements of solids volume fraction (αs) performed using Electrical Capacitance Tomography (ECT). Through the comparison with high‐speed imaging, we have shown that ECT can be used to measure the segregation behavior in cylindrical fluidized beds quantitatively. ECT measurements have been used further to quantify the effects of mixture composition, particle–diameter ratio, and superficial gas velocity on the bed segregation behavior. Dynamics of fluidization behavior is characterized using the time–evolution of local αs fluctuations, corresponding frequency distribution, and bubble size distribution. Further, a relation between the measured variance of αs fluctuations at different radial locations and corresponding flow structures under different fluidization conditions is established. The present work helps to understand dynamics of segregation and fluidization of binary mixtures and to provide a database for validation of Eulerian multifluid CFD models.

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