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Quantifying the timescales of Archean ultrahigh temperature (UHT) metamorphism is essential for constraining the style of plate tectonics on the early Earth. However, such timescales can be difficult to quantify, due to the antiquity of Archean rocks and the extreme thermal conditions of UHT metamorphism. We constrain the timescales of Archean UHT metamorphic processes recorded by a single rock sample from the Pikwitonei granulite domain (northwestern Superior Province), through the integration of two U–Pb zircon petrochronologic techniques. In this study we combine: (1) high-spatial resolution laser ablation split-stream inductively coupled mass spectrometry (LASS) on in situ zircon (in thin section) and hand-picked zircon; and (2) high-precision isotope dilution thermal ionization mass spectrometry (ID-TIMS) analyses on microsampled fragments from the same hand-picked zircon analysed by LASS. Phase equilibria modelling and Zr-in-rutile thermometry suggest the rock followed a P–T path characterized by decompression at > 960 °C, followed by near-isobaric cooling at ∼0·8 GPa. In situ LASS zircon analyses could be interpreted to record zircon growth at broadly ∼2665 Ma, though the large uncertainties on isotopic dates make potentially distinct growth episodes difficult to distinguish. ID-TIMS U–Pb dates of zircon fragments reveal a polyphase zircon growth history over a 24 Ma duration, from 2673 to 2649 Ma. Zircon trace element compositions, textures, and microstructural relationships, as well as evaluation of zircon-garnet equilibrium, suggest zircon grew during melt crystallization, after UHT decompression and garnet resorption. Variable Ti concentrations within zircon domains indicate: (1) zircon crystallized through the temperature interval of ∼875 °C to ∼730 °C, potentially in isolated rock domains with variable zircon saturation temperature; and/or (2) zircon crystallized over a narrower temperature interval in isolated rock domains with variable aTiO2 and/or aSiO2. Collectively, the data suggest the west-central Pikwitonei granulite domain reached peak UHT conditions prior to 2673 Ma, after which suprasolidus conditions in the lower crust persisted for at least 24 Ma. Such an interpretation would be impossible if based on either the LASS or ID-TIMS zircon data alone, which highlights the utility of applying both techniques in tandem to constrain metamorphic timescales in ancient UHT terranes.

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The Thompson Nickel Belt is a ca. 35 km × 400 km northeast-trending segment of the northwest margin of the Archean Superior craton in Manitoba, bounded to the west by the Paleoproterozoic Reindeer Zone. The belt was metamorphosed and deformed during the Trans-Hudson orogeny (ca. 1.9–1.7 Ga). Mineral assemblages in metamorphosed pelite, aluminous greywacke, mafic igneous rock, iron formation, and ferruginous wacke define regional metamorphic domains, separated by mineral isograds, that are subparallel to the strike of the belt and to regional-scale D3 structures. An elongate, ca. 5 km × 73 km, central zone of middle amphibolite-facies rocks is characterized by the following: muscovite-bearing mineral assemblages in pelites containing combinations of staurolite, andalusite, and sillimanite; muscovite-free, staurolite + cordierite + garnet-bearing mineral assemblages in greywackes; hornblende-bearing mineral assemblages in mafic metaigneous rocks; and grunerite-bearing mineral assemblages in iron formation. Pressure–temperature (P–T) conditions of the middle amphibolite-facies zone are ca. 550–620 °C and 3.0–5.0 kbar (1 kbar = 100 MPa), with pressure increasing to the northeast. The middle amphibolite-facies zone is bordered to the east and west by an upper amphibolite-facies zone, ca. 5 km wide on the east and ca. 3–5 km on the west. The upper amphibolite-facies zone is characterized by variably migmatitic K-feldspar + sillimanite-bearing mineral assemblages in pelites; migmatitic, garnet + cordierite + sillimanite-bearing mineral assemblages in greywackes; orthopyroxene-free, hornblende-bearing mineral assemblages in mafic rocks; and orthopyroxene-bearing mineral assemblages in iron formations. Pressure–temperature conditions of the upper amphibolite-facies zone are ca. 640–710 °C and 3.0–5.5 kbar in the southeast, and 675–755 °C and 4.5–6.0 kbar in the northwest. The outermost metamorphic zone is of the granulite facies, characterized by migmatitic garnet + cordierite + K-feldspar-bearing assemblages in pelites and greywackes, orthopyroxene + clinopyroxene ± garnet-bearing mineral assemblages in mafic rocks, and orthopyroxene + K-feldspar-bearing mineral assemblages in iron formation in which biotite is unstable. Pressure–temperature conditions of the granulite-facies zone are ca. 775–830 °C and 5.0–7.0 kbar. The P–T paths in the Thompson Nickel Belt appear to be broadly clockwise, except for some domains where they are close to isobaric. The peak P–T conditions, combined with local but widespread development of andalusite, imply relatively steep geothermal gradients of ca. 33–51 °C/km during metamorphism. Regional bathozones (domains of uniform peak-metamorphic pressure) correspond in general but not in detail with the metamorphic-facies zones. They reveal an increase in pressure towards the northeast, suggesting greater degrees of postmetamorphic exhumation in that region. Microstructural analysis suggests that peak metamorphism coincided with, and possibly outlasted, the D2 deformation event. Metamorphic isograds were deformed by D3–D4 structures. These features are consistent with a tectonic model in which the Superior craton moved in a northwest or west-northwest direction relative to the Reindeer Zone, with greatest convergence and tectonic burial occurring at the Thompson promontory.