A: SIKA is a new cold-neutron triple-axis spectrometer receiving neutrons from the cold source CG4 of the 20MW Open Pool Australian Light-water reactor. As a state-of-the-art triple-axis spectrometer, SIKA is equipped with a large double-focusing pyrolytic graphite monochromator, a multiblade pyrolytic graphite analyser and a multi-detector system. In this paper, we present the design, functions, and capabilities of SIKA, and discuss commissioning experimental results from powder and single-crystal samples to demonstrate its performance.
K: Beam-line instrumentation (beam position and profile monitors; beam-intensity monitors; bunch length monitors); Data acquisition concepts 1Corresponding author.
Magnetic structure of the Co ions in monoclinic Co 3 TeO 6 in the antiferroelectric state at 16 K has been determined by neutron powder together with single-crystal diffractions. The indices of the magnetic reflections that appear at the incommensurate positions were determined by diffractions from a single crystal, which allow to uniquely identify the magnetic modulation vector. There are two crystallographically distinct Co layers. Magnetic incommensurability appears in the Co spins in the layers comprising zigzag chains, with a magnetic modulation vector of (0.357, 0.103, 0.121) at 3 K but changes to (0.4439, 0, 0.137) at 16 K, while the Co ions in the honeycomb webs form a collinear antiferromagnetic structure. Thermal reduction rate of the Co moments in the honeycomb webs was found to be much smaller than those in the zigzag chains. Shifting of large amounts of electronic charge into the Co O bonds in the honeycomb webs on warming is used to understand the behavior.
Monovalent Na + ions have been incorporated into a multiferroic TbMnO 3 compound. Structural studies, using high-resolution neutron diffraction patterns, show that monovalent Na +-doping results in a noticeable oxygen deficiency in the compound. The alternations in crystalline and magnetic structures due to oxygen deficiency are investigated by neutron diffraction and magnetic susceptibility measurements. Na-doping turns the modulated incommensurate Mn spin structure, observed for the parent compound, into a simple commensurate one. The observed magnetic diffraction patterns agree very well with that calculated assuming a D-type arrangement for the Mn spins, with the moments pointing along the c-axis direction. No significant alternation in the ordering temperature of the Mn moments is found.
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