Preparation of reaction samples and of standard solutions for calibration All the reactants were analytical grade compounds. Hexamethyl disiloxane (HMDS, Fluka, > 98.0 %), chlorotrimethylsilane (TMCS, Fluka, > 98.0 %), and N,O-Bis(trimethylsilyl)-acetamide (BSA, Sigma, > 95.0 %), were used as silylation reagents. Gly (Aldrich, 99.0 %), FAME (methyl oleate,
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