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A gas chromatographic procedure was devised for the analysis of geometric isomers of dodecenyl acetates, tridecadienyl acetates, tetradecenyl acetates and hexadecenyl acetates. Use of diethylene glycol succinate in a 300 ft capillary column permitted the separation of nine pairs ofcis‐trans isomers and four geometric isomers of 5,9‐tridecadienyl acetate. Data are presented on the isomeric composition of alkenyl acetates prepared by three different stereospecific reactions and by elaidinization.

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