Mercurous ion was generated at 100% current efficiency from mercury-coated gold and mercury pool electrodes.
Potentiometric titrationsof halides using this generated reagent were then carried out using similar indicator
a 30-cc/min helium carrier gas flow rate, and flame ionization detectors. A 1O:l splitter divided the effluents between the flame ionization detector and the infrared cell. Ten parts went to the infrared cell and one part to the flame ionization detector. ?'he spectra were recorded on a Honeywell Visicorder recording oscillograph. Figures 10 and 11 show data obtained when this system was used to analyze 2 p1 of a synthetic mixture containing 10 z acetone, 10 z n-butyraldehyde, 10 % isovaleraldehyde, 20 z diethyl ketone, 10 z n-heptane,
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