Phenanthro[9, 10-d]imidazole derivatives were synthesized with the combinations of phenanthroquinone and benzealdehyde derivatives in the presence of ammonium acetate. The microwave-assisted protocol was investigated under solvent-free condition for 2 min (400 w). The structure of all products was studied by IR and 1 HNMR Spectroscopy. Excellent yields, short reaction times, simplicity of operation and easy separation are the advantages of this technique.
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