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Radical polymerization of methyl methacrylate initiated by the benzoyl peroxidemacrobicyclic bis ferrocenylboron capped iron(II) tris 1,2 cyclohexanedione dioximate sys tem was studied. The ferrocenyl containing macrobicyclic complex and benzoyl peroxide forms an efficient initiating system that allows one to perform the polymerization process at a high rate with substantially reduced amounts of the initiator and the metal complex component at 30-75 °С and to influence the molecular weight characteristics of poly(methyl methacry late) produced.