The yield was 5.27 g.(33.4% of the theoretical) of crude 5-chloromercuri-2thiophenecarbinol. Repeated recrystallization from hot water produced, a white powder melting at 183-185°, with decomposition.

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NotesVol. 66 added to a quinoline compound containing the trifluoromethyl group. m-Trifluoromethylphenyllithium.-To a solution of 13.5 g. (0.06 mole) of m-trifluoromethylphenyl bromide in 35 cc. of ether cooled by an ice-bath was added with stirring and over a one hour period, a. solution of 0.067 mole of nbutyllithium in 140 cc. of ether. The solution was stirred at the temperature of the ice-bath for two hours and then allowed to stand for one hour at room temperature. Color test I4 was strong, and color test IP was weak. Carbona-1.5406 and d28, 1.1475.

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