A chiral separation of R(+)-and S(-)-henzyl-3-tetrahydrofuroate (I and p-nitrobenzyl-3-tetrahydrofuroate (11) using a Chiralcel OBb (cellulose tribenzoate) column with a hexane/2-propanol ( 6 0 : 4 0 v/v) mobile phase is described. Enantiomeric purity o f R(+)-1 was evaluated using the same chromatographic conditions.
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