Treatment of Ti c14 with carboxylic acids RC02H (R = C6F5, CH2CcF5, CH20C6F5) yields a series of titanium 0x0 compounds; the X-ray molecular structure of [TiO(02CC6F5)21 reveals an octameric unit and a unique 16-mem bered T i 8 0 8 ring, with two toluene molecules encapsulated above and below the ring in the molecular cavity.
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