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A New Phosphorus Sulfide with Adamantane Structure: δ‐P4S7 By sulfur abstraction from α‐P4S9/P4S10 with triphenylphosphine a new phosphorus sulfide δ‐P4S7 with adamantane skeleton and an additional sulfur in exo‐position was identified in CS2‐solution by 31P‐NMR spectroscopy. Product distribution and 31P‐NMR parameter are given.

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