Mo4P6Si2025up from PO4 and SiO4 tetrahedra and from MoO 6 or VO6 octahedra offer new possibilities of nonstoichiometry owing to their great flexibility. Abstract. [Fe(CN)E(C~0HsN2)2](C104), M r = 519,71, orthorhombic, P212~21, a = 10.950 (6), b = 11.941 (2), c=16.912(4)/1., U=2211
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