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The 16alpha,17alpha-epoxy-16beta-methylandrostane-17beta-carbothioic acid 2b rearranges in solution at ambient temperature to the 17beta-mercapto-16beta-methylandrostane-17alpha,16alpha-carbolactone 6a, possibly via the spirocyclic alpha-thiolactone 5.

Rearrangement of a 16α,17α-Epoxy-16β-methylandrostane-17βcarbothioic Acid to a 17β-Mercapto-16β-methylandrostane-17α,16αcarbolac tone. -In solution at ambient temperature the acid (I) undergoes facile rearrangement to the lactone (II). -(BAIN, BRIAN M.; PHILLIPPS, GORDON H.; PROCOPIOU, PANAYIOTIS A.; STEEPLES, IAN P.; UPTON, RICHARD J.; J.

ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable via the “References” option.