Thin films of (BEDT-TTF)2Cu(NCS)2 are prepared by the electrochemical oxidation of BEDT-TTF at a large current density. The films are composed of numerous platelets, which are set on edge and loosely packed on the anodes. The X-ray diffraction suggests that the product contains both amorphous regions and κ-type and other crystals. The ESR and conductivity are discussed in terms of the presence of amorphous regions.
Allyl diphenyl phosphate[ADP] reacted with a large excess of aromatic compounds possessing electrondonating group in the presence of boron trifluoride etherate under mild experimental conditions to give selectively the corresponding monoallylated compounds in the yield of 40–60%.
Allyl‐diphenylphosphat (I) reagiert in Gegenwart von Borfluoridätherat mit einem großen Überschuß an Aromaten in Ausbeuten von 40‐60% zu monoallylierten Verbindungen.
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