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In this mode the intensities of only four selected mass peaks are measured.(31) (a) F. H.

The same procedure as above was used with 11.5 mL of Ac20, 2.5 mL of oxide-free HN03, and a solution of 2.0 g of the amine hydrochloride in 2 mL of AcOH. A workup as above gave 0.51 g of dimethylnitramine as a first crop. Further concentration gave another 0.21 g (total yield 55%).

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Die Spaltung der Arylsulfonate (I) durch Naphthalin‐Radikalanionen (II) liefert im wesentlichen die Alkohole (III) neben geringen Anteilen an den Kohlenwasserstoffen (IV); aus Neopentyl‐p‐toluolsulfonat entsteht zudem das tert.‐Butyl‐dihydronaphthalin (VI).