The tungsten trioxide (WO3) and copper(II) oxide (CuO) photoelectrodes have been fabricated from acidic aqueous solution of peroxy-tungstate and basic aqueous solution of copper sulphate-lactic acid respectively, by electrodeposition method. The samples produced were calcined at 450 °C for 30 minutes before the deposition of second layer. The CuO was layered on WO3 sample by electrodeposition of basic aqueous solution of copper sulphate-lactic acid, followed by annealing process at 450 °C for 30 minutes. On the other hand, the WO3 layer was casted onto CuO sample by sol-gel method and it was annealed at 450 °C for 30 minutes. The resulting samples were then characterized by XRD to confirm their structures. Photoelectrochemical characterization of the WO3, CuO and WO3-CuO bilayer photoelectrodes were carried out under 100 W xenon light illumination, in 0.5 M sodium sulphate solution with saturated calomel electrode (SCE) reference electrode and platinum counter electrode. The PEC stability of the electrodes was evaluated at -0.7 V vs SCE under irradiated condition.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.