In this paper, we report on the construction of a novel test facility for evaluating catalytic processes at high temperature and high pressure. The design features make the facility well-suited for highly controlled studies of hydrothermal conversion of real biomasses with complex composition. The proof of concept is provided by bio-oil production from (i) Dried Distiller's Grains with Solubles (DDGS), the results serving to illustrate catalyst performance, and (ii) spent coffee grounds, which exemplify constituent analysis of the as-produced bio-oil. Both studies were carried out under near-critical conditions using both homogeneous and heterogeneous catalysts.
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