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Supplementary Material Available: Crystallographic data including tables of the atomic positional and thermal parameters and bond angles for 10 (4 pages). Ordering information is given on any current masthead page.

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Benzyl selenocyanates can be made from the corresponding benzylic bromides or chlorides in 30-60 minutes using acetonitrile as a solvent. The products may be obtained pure in satisfactory yields without recourse to chromatography.