We report the precise postsynthetic control of the composition of β‐Fe1+xSe by electrochemistry with simultaneous tracking of the associated structural changes via in situ synchrotron X‐ray diffraction. We access the full phase width of 0.01
Die Zusammensetzung von β‐Fe1+xSe wurde postsynthetisch in elektrochemischen Experimenten variiert, mit gleichzeitiger Analyse der strukturellen Veränderungen via In‐situ‐Synchrotron‐Röntgenbeugung. Die gesamte Phasenbreite von 0.01
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