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The composition dependence of quadrupole splitting (QS) in Zn‐substituted Cd‐ferrites has been investigated using the Mössbauer effect measurements. Mössbauer spectra of 57Fe in Cd1—xZnxFe2O4 (x = 0, 0.25, 0.50, 0.75, 1.0) ferrite systems were taken at room temperature. It is found that both calculated and experimental values of QS vary linearly with the increase of Zn2+ cations and also have a good agreement between themselves. The isomer shift (IS) for all probable site occupancies remains the same in all compositions.

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