An X-ray structural study of the crystals isolated from the solutions obtained by the reaction of Ba metal with Ti(OPri)4 in isopropyl alcohol has been carried out; the crystals of the compound, which is a precursor for the synthesis of BaTi03, contain molecules of two different kinds [Ba4Ti404(0R)16(ROH)4] and [Ba4Ti404(0R)16(ROH)3], where R = Pri.
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