The soil samples from Mambila Plateau were analyzed to determine the physicochemical properties of elements present by energy dispersive X-Ray Fluorescence. The physical and chemical parameters determined were colour, pH, electrical conductivity, specific gravity and elemental identifications of Cr 2 O 3 , CuO, NiO and V 2 O 5 respectively. The pH values for soils of the study area are high between 3.96-4.30 being acidic, electrical conductivity values ranged from 81.79 -238 mS/cm with higher electrical conductivity value at N 1 having 238 mS/cm and lower electrical conductivity at S 1 81.79 uS/cm respectively. The soil are yellow, red and gray; with hue steps of 2.5YR, 5YR, 7.5YR, and 10YR, a step values between 3-7 and the chroma range of 1-6. The specific gravity which also is the relative density range from 2.00-2.50. The percentage elemental contents identified for trace elements decreased in the order V 2 O 5 > Cr 2 O 3 >NiO > CuO. The highest percentage concentration of element found was V 2 O 5 at N 4 0.29% while, CuO showed minimum concentration of 0.01%. The entire soils indicated high acidity levels due to the pH results tested, with spatial variation of the elements oxides contents higher at