The article describes a new and effective synthesis of pure imido-bis(sulfuric acid) dihalogenides (halogenide ϭ F, Cl) and the potassium salt of imido-bis(sulfuric acid) difluoride, KN(SO 2 F) 2 .
Abstract:The ternary chloride Na 3 MoCl 6 is obtained as red crystals from a disproportionation reaction of molybdenum dichloride, {Mo 6 }Cl 12 , in an acidic NaCl/AlCl 3 melt at 350 °C. The crystal structure (trigonal, P-31c, a = 687.1(1), c = 1225.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.