X-ray powder diffraction data for a new potassium sodium silicate Na1.3K0.7Si2O5are reported. The sample was prepared by calcining a mixture of NaOH, KOH, and sodium silicate (SiO2/Na2O=3.54, moisture content=60%) at 873 K for 2 h. The crystallographic data obtained by using the whole-powder-pattern decomposition method are Na1.3K0.7Si2O5, monoclinic, P21/c, a=4.8426(1) Å,b= 8.6892(2) Å,c= 11.9686(3) Å,β=90.373(2)°,V=503.60(2) Å3,Z=4,Dx= 2.51 g/cm3.
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