The investigation was concentrated on preparation of bioactive pure cordierite ceramic and evaluate the phase transformation which excepted to form during sintering process. Cordierite prepare by chemical co precipitation, integrated Cordierite gel with water-based sol–gel which begin essentially from Alumina Al2O3, magnesium oxide MgO and silicon oxide SiO2. Different specimens were fabricated with various weight percentage of Al2O3, Mgo and SiO2 powders. All specimens were prepared in cylindrical shape by using hydraulic press at pressure of 4 bar with holding time at this pressure for 30 minutes. Firing presses achieve at 10000C and 12500C with 2 hour holding time. The characterization of microstructure has been done by using Field Emission Scanning Electron Microscope (FESEM), which revealed homogenous distribution of the compounds with few porosities. The x-ray diffraction for phase transformation which occur during sintering process. The structure analysis of specimens shows at 1250°C cordierite phase form, also the results are shown formation of cristobalite, spinel, protoestatite and corundum with cordierite phase.
The study concentration on the fabricate of bioactive behavior of pure cordierite system and investigate the structure of phase transformation and physical characteristics. cordierite powders were synthesized by chemical coprecipitation, combined Cordierite gel with water-based sol–gel which begin fundamental from magnesium oxide MgO, Alumina Al2O3 and silicon oxide SiO2. Five specimens were prepared with different weight percentage of Mgo, Al2O3 and SiO2 powders. cylindrical shape samples were press by hydraulic press at 4 bar for 30 minutes. All specimens were sintered at 1250 0C.The microstructure examination of specimens was carried out using Field Emission Scanning Electron Microscope (FESEM), x-ray diffraction (XRD) and particle size analysis The analysis revealed cordierite phase formation at 1250 °C, and the intense peaks were identified for composites S4 and S5. The results also indicated the formation of spinel, cristobalite, corundum, protoestatite and cordierite for all the specimens.
This study focused on the production of bioactive pure cordierite ceramic and the evaluation of its bioactivity by immersing it in simulated bodily fluid (SBF) and coating it on CP-Ti utilizing the dip coating Procedure. Cordierite is created by chemical coprecipitation, which involves combining Cordierite gel with a water-based sol-gel composed of Alumina Al2O3, magnesium oxide MgO, and silicon oxide SiO2. They used a hydraulic press to form cordierite into a cylindrical shape with a pressure of 4 bar and a holding time of 30 minutes at this pressure. Firing presses reach temperatures of 1250 Co and have a holding time of 2 hours. A Field Emission Scanning Electron Microscope (FESEM) was used to examine the microstructure, which revealed a homogenous distribution of the compounds with negligible porosities. The phase transitions that cur during the sintering Process is studied using X-ray diffraction (XRD). The structural investigation of specimens revealed the formation of the cordierite phase at 1250 Co, as well as the development of cristobalite, spinel, protoestatite, and corundum with cordierite phase. The dip coating Procedure was utilized to cover commercial pure titanium (CP-Ti) samples with cordierite powder. CP and Tafel exploration tests show that coated CP-Ti has superior passivation than uncoated Substrate. By comparing the findings of uncoated and coated CP-Ti, this paper concludes that the cordierite system acts as a good passivation layer.
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