This research work focus on the formation of AA2024-carbon nanotubes-silicon hybrid metal matrixcomposites. Structure morphology, structural characterization, elemental identification and dielectric properties of AA 2024 in the presence of carbon nanotubes, silicon andits combinations at various proportions was evaluated using SEM, XRD, EDX and Hioki 3532-50 LCR Hi-Tester. A two-stage stir casting method was used for the fabrication of AA2024 hybrid metal matrix composites. It was observed that the size of the AA 2024 + 4% CNT + 2% Si composite wasfound to be 23.6 nm, this shows enhanced results than other composites prepared. Dielectric properties of composites were characterized as a function of composition and frequency. It was found that the dielectric constant, dielectric loss and dissipation factor decreases smoothly with an increase of reinforcements and also frequency.