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The reaction of thiolesters with titanocene alkylidenes prepared by the treatment of thioacetals with the low valent titanium species Cp2Ti[P(OEt)3]2 produced the corresponding alkenyl sulfides in good yields with moderate to good Z stereoselectivity.

hydrocarbons hydrocarbons (benzene compounds) Q 0080 -085Titanocene(II)-Promoted Desulfurizative Tertiary Alkylation of 1,3-Bis(phenylthio)alk-1-enes and β,γ-Unsaturated Thioacetals.-The title compounds undergo desulfurization with the low-valent titanium species Cp 2 Ti[P(O-Et) 3 ] 2 .

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