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Cobalt oxide doped in polyaniline nanocomposite were prepared with various weight percentages by in situ polymerization method and thin films by solvent casting method,for preparation of composite using aniline, ammonium per sulfate, and Cobalt oxide as starting materials. The temperature dependent conductivity behavior of PANI/ Cobalt oxide composites have been studied. The formation of PANI and PANI/ Cobalt oxide composites with regards to the structural and microstructural properties of the materials were investigated by SEM techniques. The conductivity of Pure PANI and its composites have been measured.

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