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Recent investigations have highlighted the multi-resolution and high throughput characteristics of the spherical indentation experimental and analysis protocols. In the present work, we further demonstrate the capabilities of these protocols for reliably extracting indentation stress-strain (ISS) responses from the microscale constituents as well as the bulk scale of dual phase materials exhibiting bimodal microstructures. Specifically, we focus on bimodal microstructures produced in an α–β Ti6242 sample. Combining the multi-resolution indentation responses with microstructural statistics gathered from the segmentation of back-scattered electron images from the scanning electron microscope allowed for a critical experimental evaluation of the commonly utilized Rule of Mixtures based composite model for the elastic stiffness and plastic yield strength of the sample. The indentation and image analyses protocols described in this paper offer novel research avenues for the systematic development and critical experimental validation of composite material models.

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