3β‐Hydroxysteroide wie z.B. die Verbindungen (I) und (III) mit elektronegativer Substitution der 5a‐Stellung werden durch Bleitetraacetat in Gegenwart von Calciumcarbonat und einer Spur Benzoylperoxid zu 3β,19‐Oxidosteroiden (II) und (IV) oxidiert.
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