The quantitative recovery and structural alterations of aldehydes liberated from O‐alk‐1‐enyl glycerols on thin layer chromatographic layers have been evaluated by using14C‐labeled fatty aldehydes and chromatography. The results led to the development of a quantitative procedure for isolating the aldehydes produced from O‐alk‐1‐enyl glycerols by shaking an ethereal solution of the ether‐linked lipids with concentrated hydrochloric acid. The procedure is rapid and silicic acid does not interfere.

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