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Herein, the structure and magnetic properties of the breathing pyrochlore compound LiInCr4−xFexO8 (x = 0, 0.2, 0.4, 0.5) are reported. Raman scattering experiments show the hardening behavior of the active mode induced by the increased ionic masses and bond strength. The long‐range antiferromagnetic order and spin‐gap state of parent samples are found to be suppressed with the increasing Fe content. The average magnetic exchange couplings are strongly antiferromagnetic and systematically enhanced with substitution. Bulk magnetization data of substituted samples show weak ferromagnetic interaction and occurrence of a spin‐glass‐like transition at high Fe contents.

FeSi/1wt% glass soft magnetic composites are prepared by mechanically mixing, compacting, and annealing, their morphology is examined by SEM, and their magnetic properties are measured by MPMS and B-H analyzer. The morphology of SEM shows that when the annealing temperature is higher than the melting point of the glass, the glass particles between the FeSi balls are deformed into flakes. The sample has higher saturation magnetization and lower power loss. The magnetic permeability and mechanical strength of the sample increase with the increase of annealing temperature, but the best power loss characteristics emerge at annealing temperature of 400 °C.

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