NOTES 1671 trichloride (3.76 g., 0.032 mole) in 20 ml. of methylene chloride at -80°. After allowing the mixture to warm, the solvent was removed at the pump. The yellow-orange solid residue was recrystallized from benzene and then from carbon disulfide. Infrared analysis indicated that the compound was triphenylchloromethane. This was confirmed by hydrolyzing a weighed sample in aqueous acetone and titrating the hydrochloric acid liberated.

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