Bi-2212 superconducting single crystals were grown by the travelling solvent floating zone method at different oxygen ambient pressures. Electron probe micro-analysis showed a systematic increase of the Sr/Ca ratio in the as-grown crystals with increasing oxygen ambient pressure and a maximal superconducting transition temperature of Tc~onset= 95 K, and ziT= 1.5 K was obtained for crystals grown at an oxygen ambient pressure of 200 kPa. Thermogravimetric and post-annealing experiments in air at 500 and 800°Chave shown that the oxygen content and the Tconset values in the crystal do not depend only on the annealing temperature, but also on its chemical composition. The in-field current density J~measured at 5 K on crystals grown at 200 kPa oxygen ambient pressure was considerably smaller than that of crystals grown in air.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.