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~ ~ ~~~~~~~~~~~Synthesis of Fungicidal (1H-l,2,4-Triazol-l-yl-methyl)silanes and -siloxanesThe synthesis of FlusilazoleTM (la) was substantially impro-sponding silanol hydrochlorides and further treated with ved by thorough exclusion of oxygen nucleophiles in the re-functional, linear oligodimethylsiloxanes or secondly from action of (chloromethyl)bis(4-fluorophenyl)methylsilane with a,a-diaryl-a-(chloromethy1)siloxanes and 1 -(trimethylsilyl)-sodium 1 H-1,2,4-triazolide. New a,a-diaryl-a-(lH-1,2,4-tri-lH-1,2,4-triazole. The siloxane 4 containing a triazolylmethyl azol-1 -yl-methy1)siloxanes 3 were obtained firstly from group and additionally silicofunctional coupling groups diaryl( 1 H-1,2,4-triazol-l-yl-methyl)silanols or -silanolates, could be synthesized by hydrosilylation of an a-triazolylmewhich were prepared by different methods from the corre-thyl-o-vinylsiloxane with triethoxysilane.

1996organo-silicon compounds, nonmetal heterocycles organo-silicon compounds, nonmetal heterocycles S 0067 -192Synthesis, Solid-State Structure, and Reduction of 1,1-Dichloro-2,3,4, 5-tetramethylsilole.--(BANKWITZ, U.; SOHN, H.; POWELL, D. R.; WEST, R.; J. Organomet. Chem. 499 (1995) 1-2, C7-C9; Dep. Chem., Univ. Wis., Madison, WI 53706, USA; EN)

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