A facile method for reduction of
textile effluents (TEff) using
fluorescent nitrogen-doped carbon dots (N-CDs) has been developed
and reported here. The synthesis of N-CDs was done by a hydrothermal
carbonization method using the aqueous extract of
Phyllanthus
emblica
(
P. emblica
) fruit as a carbon source and aq NH
3
as a nitrogen dopant.
Various analytical techniques have been employed for the characterization
of N-CDs. The size of the synthesized N-CDs was found to be 4.08 nm,
which was confirmed by high-resolution transmission electron microscopy
analysis. The graphitic character of the N-CDs was studied by using
selected area energy diffraction pattern and Raman spectroscopy studies.
Under the excitation of 320 nm, an intense blue fluorescence was emitted
by N-CDs of around 400 nm. From the obtained results of energy-dispersive
spectrometry, EDAX, and Fourier transform infrared studies, it was
confirmed that nitrogen was doped over the N-CD surface. Finally,
the catalytic ability of NaBH
4
was found to be enhanced
remarkably by the synthesized CDs in the detoxification of TEff.
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