Heat treatment of graphene oxide (GO) with ammonia flow at various temperatures resulted in different distribution of nitrogen species. Synchrotron based X-ray absorption near-edge structure (XANES) spectroscopy provides unambiguous evidence for the presence of three nitrogen species. The Pt/NG-800 composite exhibits outstanding electrocatalytic activity for methanol oxidation.

Reduced graphene oxide (RGO) was synthesized under H(2)/Ar treatment from 100 °C to 900 °C. RGO-300 shows excellent sensitivity to H(2) and a dual sensing mode was observed. The balance between the chemical adsorption capacity and electronic conductivity, and the dominance of either electrons or holes are the key factors.

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